2. Standard issued by the Ministry of Traditional Chinese Medicine 2. 1 Pinyin name: Houtong Jiedu Pill
2.2 standard number WS3B 124492
2.3 prescription bezoar 45g borneol 30g realgar 30g toad venom 30g indigo 30g Sophora tonkinensis 60g white grass 45g
2.4 The preparation of the above-mentioned seven herbs includes grinding or pulverizing realgar into animal powder, grinding bezoar and other four herbs into fine powder (adding water into ground Venenum Bufonis to make Venenum Bufonis paste for preservation), mixing with the above powders, sieving, mixing, adding water to make pills, and drying at low temperature. Pulverizing Venenum Bufonis, coating Venenum Bufonis slurry and Venenum Bufonis powder, drying at low temperature, and polishing.
2.5 Features This product is a water pill with bright ink color; It is fragrant, bitter and slightly numb.
2.6 Identification (1) Take a little powder of this product, which is slightly sublimated. The sublimate is dissolved with 1 ~ 2 drops of ethanol, and then added with 1 ~ 2 drops of new vanillin sulfuric acid solution, which turns purple.
(2) Take 0 or so. Take 3g of this product, grind it in a mortar, add water to moisten it, add 3ml of nitric acid solution saturated with potassium chlorate, fully grind it, and then filter it. Add 0.5 ml of barium chloride test solution to the filtrate to produce a white precipitate. After standing, discard the upper acid solution, add 2ml of water, shake well, and the precipitate will not dissolve.
(3) Take 0 or so. Take 2g of this product, grind it, add 5ml of ethanol, fully grind it, filter it, and concentrate the filtrate to 65438±0ml as the test solution. In addition, cholic acid and hyodeoxycholic acid were taken as reference substances, and ethanol was added to prepare a mixed solution containing 2mg per kloc-0/ml as reference substance solution. According to the thin-layer chromatography test (page 57 of the appendix), absorb 2μl of each of the above two solutions, respectively spot them on the same silica gel G thin-layer plate, use the upper solution of hexane, acetic acid, ethyl acetate and methanol (20:25:2:3) as the developing agent, unfold, take them out, air dry them, and spray them with 10% sulfuric acid ethanol solution. Bake at 65438 005℃ for about 65438 00 minutes, and check under ultraviolet lamp (365nm). In the chromatogram of the test sample, fluorescent spots with the same color appear in the position corresponding to the chromatogram of the control sample.
(4) Take 0 or so. Take 3g of this product, grind it, add 5ml of chloroform, grind it fully, filter it, and concentrate the filtrate to 65438±0ml as the test solution. Indigo and indirubin were taken as reference substances, and chloroform was added to make a mixed solution containing 1ml as reference substance solution. According to the thin-layer chromatography test (Appendix 57), absorb 5 ~ 10μ l of the above two solutions, spot them on the same silica gel G thin-layer plate, use phenyl chloroform acetone (5:4: 1) as the developing agent, unfold and take them out, and in the chromatogram of the test sample, the spots with the same color will appear in the original position corresponding to the chromatogram of the control sample. ?
2.7 In addition to the "dissolution time limit", it should meet the requirements of pills (Appendix? Page).
2.8 Functions and indications: clearing away heat and toxic materials, diminishing inflammation and relieving pain. It can be used for treating laryngitis, furuncle, furuncle swelling, and sores on mouth and tongue.
2.9 Usage and dosage: 5 ~ 10 capsules each time, 3 times a day; Children should be reduced.
2. 10 Pregnant women should be careful.
2. 1 1 specifications Each 10 capsule weighs 0. 03g。
2. 12 storage seal.
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