2. Standard issued by the Ministry of Traditional Chinese Medicine 2. 1 Pinyin name Chanlongdingchuan mixture
2.2 standard number ws3-b-4048-98
2.3 Prescription Ephedra, Toad, Lumbricus, Schisandra, Epimedium, Ramulus Cinnamomi, Red Ginseng, Radix Astragali, Radix Paeoniae Alba, Pericarpium Citri Tangerinae, Pinellia ternata, Almond Dried Ginger, Pig Bile, Radix Glycyrrhizae, Radix Platycodi and Perillae Leaves.
2.4 The preparation method of the above 19 kinds of medicines except pig bile, dried ginger and toad, ginseng and earthworm are washed, crushed as appropriate, and decocted with other 14 kinds of medicines such as ephedra in water for three times, the first time and the second time are 2 hours each, and the third time is 1 hour. Mixing decoctions, filtering, and concentrating the filtrate to the same amount as the original medicinal materials. Chop Bufo bufo gargarizans, decoct with pig bile and dried ginger in water for three times, each time for 65,438+/-0 hours, combine decoctions, filter, combine filtrate with the above standby solution, concentrate to the same amount as the original medicinal materials, add ethanol to make the alcohol content reach 70%, stand for 36 hours, take supernatant, and recover ethanol until it has no alcohol smell. In addition, 0. Dissolve 77g stevioside and 3g sodium benzoate in a small amount of distilled water, then add them into the above liquid medicine, add water to the total amount of 1000ml, stir evenly, refrigerate for 24 hours, absorb the supernatant, and make capsules.
2.5 Properties This product is a brown-red clear liquid; It tastes bitter.
2.6 Identification (1) Put this product 10ml in a test tube, and foam will be generated after strong shaking, and it will not disappear within10min.
(2) Take this product 10ml, put it in a separatory funnel, adjust the pH value to 12 with concentrated ammonia water, shake well, extract it with chloroform for three times, each time 10ml, combine chloroform solutions, and adjust the pH value to/kloc with dilute hydrochloric acid (3→ 10). Another ephedrine hydrochloride reference substance was added with methanol to prepare a solution containing 1 mg per 1 ml as the reference substance solution. According to the thin-layer chromatography test (Appendix ⅵ b), absorb 5 ~10 μ l of the above two solutions, respectively spot them on the same silica gel G thin-layer plate with sodium carboxymethylcellulose as adhesive, and use chloroform-methanol-concentrated ammonia water test solution (10: 2: 0. 1) as developing agent, unfold and take them out. In the chromatogram of the test sample, spots with the same color appear in the position corresponding to the chromatogram of the control sample.
2.7 Check that the relative density should not be less than 1.04 (Appendix VII a). The pH value should be 4.0 ~ 6.0 (appendix VII g). Others shall comply with the relevant regulations in the mixture (Appendix I J).
2.8 Indications: dispelling cold and resolving phlegm, nourishing lung and kidney, relieving cough and asthma. It is used for chronic bronchitis caused by lung and kidney qi deficiency and bronchial asthma caused by deficiency of cold and phlegm.
2.9 Usage and dosage: 10ml once, three times a day.
2. 10 Pay attention to patients with lung dryness and cough and asthma caused by lung heat and yin deficiency. Alcohol and smoking should be avoided during medication. Shake well when taking.
2. 1 1 specification 100ml per bottle.
2. 12 stored in a cool and dry place and sealed.
Draft by Institute for Drug Control of Inner Mongolia Autonomous Region
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